Seeking: Acetic acid recovery system for use with industrial effluent stream

  • Anonymous Organization
  • From United States
  • Responsive
  • Deadline completed
    The submission process for new proposals is closed. Proposals submitted before the deadline will follow the standard evaluation process.

Desired outcome

Our new chemical facility produces a substantial quantity of acetic acid as a byproduct, which requires environmental recovery. However, wastewater treatment is expensive, and acetic acid has a value as a product if we can recover it in a high-purity form (+99.5%).

Organization from United States
Organization from United States

Details of the Technology Call

BACKGROUND

Our process effluent stream contains low concentrations of acetic acid (10% to 15%, without other impurities). However, recovering it from the wastewater stream using current treatment technology is very costly. We want to recover the acetic acid using a more economical process. Recovered acetic acid must be of high purity (minimum 99.5%) to remain commercially viable.

There appears to be two basic options:

1) Recover acetic acid from the effluent stream using acetic acid distillation and solvent extraction. This option requires little energy consumption, but using a solvent increases wastewater treatment costs.

2) Use a process that changes acetic acid to ethyl acetate, and then recover the ethyl acetate (also a valuable commercial compound). This is a complex process.
Ideally, we would find a recovery process for acetic acid. It is possible to recover 20,000 tons/year of pure acetic acid from our process.

CONSTRAINTS

Your proposed system must offer:
o economical methods of recovery
o high-purity acetic acid (+99.5%)
o technology ready for commercialization (we would like to apply your proposed process as quickly as possible)

POSSIBLE SOLUTION AREAS

Industries producing terephthalic acid. The terephthalic acid production process also produces acetic acid a byproduct. We may be able to learn from their acetic acid recovery experience.

Solvent extraction and distillation technologies (we are using CYANEX923 as solvent).

Companies practicing reaction distillation.

Field Of Use and Intended Application
Economical recovery of acetic acid.

Desired Outcome
We would like to find an economical recovery process, or an engineering company with extensive experience in acetic acid recovery, especially with experience in using CYANEX923 solvent. We currently are testing an extraction process using CYNEX923(CYTEC) solvent.

Previously Attempted Solutions
We are currently testing a solvent extraction and distillation system.

Related Keywords

  • Biological Sciences
  • Industrial Technologies
  • Physical Sciences and Exact Sciences
  • Protecting Man and Environment
  • Genetic Engineering / Molecular Biology
  • Industrial Products
  • Medical Health related
  • acetic acid
  • industrial effluent

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